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2,3-Epoxypropyl 4'-methoxyphenyl ether → HCID 14739881、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2,3-Epoxypropyl 4'-methoxyphenyl ether | HCID 16646 | — |
| 反応物 | N-(2-Aminoethyl)-4-(1H-imidazol-1-yl)benzamide | HCID 14664358 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | HCID 14739881 | HCID 14739881 | — |
反応手順
To a solution of 2.39 g (13.2 mmol) 1,2-epoxy-3-(4-methoxyphenoxy)propane in 25 mL methanol is added 3.05 g (13.2 g) N-(2-aminoethyl)-4-(1H-imidazol-1-yl)benzamide. The reaction mixture is stirred under a nitrogen atmosphere for 24 h. After this time, the precipitate is collected and recrystallized from ethanol to provide the title compound.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05051423 |
| 出典データセット | uspto-grants-1991_09 |
| ORD ID | ord-38e8628e4cb44652858f6f795a33044a |
| 出典メモ | uspto-grants-1991_09 |