HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → 4-(3-Methoxyphenyl)-1-(phenylmethyl)-2-piperazinecarboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 2,3-Dibromopropionamide | HCID 85798 | — |
| Reactant | N-(3-methoxyphenyl)-N'-(phenylmethyl)-1,2-ethanediamine | HCID 14998753 | — |
| Product | 4-(3-Methoxyphenyl)-1-(phenylmethyl)-2-piperazinecarboxamide | HCID 14998754 | — |
Reaction Steps
In a manner similar to Preparation 1, react N-(3-methoxyphenyl)-N'-(phenylmethyl)-1,2-ethanediamine (16 g, 63 mmol) with 2,3-dibromopropanamide (29 g, 126 mmol) and triethylamine (25 g, 0.25mol) to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05051422 |
| Source dataset | uspto-grants-1991_09 |
| ORD ID | ord-aab76a66a86f430f84704cda31947069 |
| Source note | uspto-grants-1991_09 |