HRID728941

反应详情

EQUATION

反应方程式

HRID 728941 的结构方程式

PROCEDURE

实验过程

To 4-(2-methyl-1H-imidazole-1-yl)benzenemethanol add thionyl chloride. Monitor the progress of the reaction by thin-layer chromatography. Upon completion remove the excess thionyl chloride in vacuo. Partition the residue between 1N NaOH and CH2Cl2. Separate and dry the organic layer. Remove the solvent in vacuo to obtain the title compound.

WORKUP

后处理

  1. customMonitor the progress of the reaction by thin-layer chromatography
  2. customUpon completion remove the excess thionyl chloride in vacuo
  3. customPartition the residue between 1N NaOH and CH2Cl2
  4. customSeparate
  5. customdry the organic layer
  6. customRemove the solvent in vacuo