HRID728941
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
PROCEDURE
实验过程
To 4-(2-methyl-1H-imidazole-1-yl)benzenemethanol add thionyl chloride. Monitor the progress of the reaction by thin-layer chromatography. Upon completion remove the excess thionyl chloride in vacuo. Partition the residue between 1N NaOH and CH2Cl2. Separate and dry the organic layer. Remove the solvent in vacuo to obtain the title compound.
WORKUP
后处理
- customMonitor the progress of the reaction by thin-layer chromatography
- customUpon completion remove the excess thionyl chloride in vacuo
- customPartition the residue between 1N NaOH and CH2Cl2
- customSeparate
- customdry the organic layer
- customRemove the solvent in vacuo