huagongshe.com
HRID729014

反应详情

EQUATION

反应方程式

HRID 729014 的结构方程式

REACTANTS

反应物

3
结构：[Na+].[OH-]
HCID14798

Sodium Hydroxide

HNaO

结构：CCOC(=O)CCN
HCID419889

Ethyl 3-aminopropanoate

C5H11NO2

结构：C=CCc1cc(CC(N)=O)ccc1OCC1CO1
HCID54437989

未命名化合物

PRODUCTS

生成物

1
结构：C=CCc1cc(CC(N)=O)ccc1OCC(O)CNCCC(=O)OCC
HCID67929459

ethyl N-[3-(2-allyl-4-carbamoylmethylphenoxy)-2-hydroxypropyl]-3-aminopropanoate

C19H28N2O5

PROCEDURE

实验过程

This compound was prepared in accordance with Example 1 using 10.8 g of thehydrochloride of ethyl 3-aminopropanoate, 11.6 g of 3-allyl-4-(2,3-epoxypropoxy)phenylacetamide, and 2.84 g NaOH. The crude product was crystallized from ethyl acetate. Yield 1.7 g. Melting point 98° C. (base). The structure was determined using NMR and equivalent weight.

WORKUP

后处理

  1. customThe crude product was crystallized from ethyl acetate