HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 729024Generated: October 31, 2026
Sodium Hydroxide → HCID 178420092, compound
https://huagongshe.com/reaction/729024
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Ammonium Chloride | HCID 25517 | — |
| Reactant | Sodium Azide | HCID 33557 | — |
| Reactant | HCID 14800671 | HCID 14800671 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 178420092 | HCID 178420092 | — |
Reaction Steps
A mixture of sodium azide (0.03 mol), ammonium chloride (0.03 mol) and 3-(4-(2-quinolinylmethyloxy)benzyl)benzonitrile (0.01 mol) in dimethylformamide (20 ml) are heated at 100° C. for 18 hours. The reaction is poured into aqueous 10% sodium hydroxide solution and washed with ethyl acetate. The crystalline product is isolated by acidification and filtration to obtain 5-(3-(4-(2-quinolinylmethyloxy)benzyl)phenyl)tetrazole.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05051427 |
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| Source dataset | uspto-grants-1991_09 |
|---|
| ORD ID | ord-1a5e027924b64ee89e7d2967de930663 |
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| Source note | uspto-grants-1991_09 |
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