HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 14995019, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | HCID 14995018 | HCID 14995018 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 14995019 | HCID 14995019 | — |
Reaction Steps
To methanesulfonyl chloride (0.002 mol) and triethylamine (0.002 mol) in dichloromethane (40 ml) at 0° C. is added 3-(4-(2-quinolinylmethyloxy)benzyl)benzyl alcohol (0.0018 mol) in dichloromethane (40 ml) dropwise. After 24 hours, the reaction mixture is washed with water, dried and evaporated to give 3-(4-(2-quinolinylmethyloxy)benzyl)benzyl alcohol mesylate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05051427 |
| Source dataset | uspto-grants-1991_09 |
| ORD ID | ord-5c58d14ece984d08837e7a813c86aa14 |
| Source note | uspto-grants-1991_09 |