Ammonia → HCID 178428279, compound

HRID 729181Notes

Reaction equation

HRID 729181 reaction equation
CS(O)(=O)=O.CS(O)(=O)=O.[NH2:11][C:12]1[C:19](=[O:20])[N:15]2[CH2:16][CH2:17][CH2:18][N:14]2[C:13]=1[NH2:21].[NH2:22][C:23]1[C:24]([Cl:31])=[C:25]([OH:30])[C:26]([CH3:29])=[CH:27][CH:28]=1.N.OO>O.C(O)C>[NH2:21][C:13]1[N:14]2[CH2:18][CH2:17][CH2:16][N:15]2[C:19](=[O:20])[C:12]=1/[N:11]=[C:28]1/[C:23]([NH2:22])=[C:24]([Cl:31])[C:25](=[O:30])[C:26]([CH3:29])=[CH:27]/1

Participants

7

Reactant 4

HCID 222AmmoniaHCID 784Hydrogen PeroxideHCID 1576415-Amino-6-Chloro-o-CresolHCID 715878212,3-Diaminodihydropyrazolo pyrazolone dimethosulfonate

Product 1

HCID 178428279HCID 178428279, compound

Reagents, catalysts & solvents 2

HCID 702EthanolSolventHCID 962WaterSolvent

Procedure

0.58 mmol of 2,3-diamino-6,7-dihydro-1H,5H-pyrazolo[1,2-a]pyrazol-1-one dimethane sulphonate was dissolved in a mixture of water and ethanol (7.5 ml/1.5 ml). This solution was admixed with 0.58 mmol of 3-amino-2-chloro-6-methylphenol, then with 1.8 ml of concentrated aqueous ammonia, then with 9 ml of hydrogen peroxide.

Sources & evidence

ORD record
ord-e28c626682fe44c0827f13e48428b518
Source dataset
uspto-grants-2009_09
Patent number
US07582123B2

Reaction notes

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