Ammonia → HCID 178493061, compound

HRID 729183Notes

Reaction equation

HRID 729183 reaction equation
CS(O)(=O)=O.CS(O)(=O)=O.[NH2:11][C:12]1[C:19](=[O:20])[N:15]2[CH2:16][CH2:17][CH2:18][N:14]2[C:13]=1[NH2:21].[OH:22][CH2:23][CH2:24][NH:25][C:26]1[CH:27]=[CH:28][C:29]([O:33][CH3:34])=[C:30](O)[CH:31]=1.[NH3:35].OO>O.C(O)C>[NH2:21][C:13]1[N:14]2[CH2:18][CH2:17][CH2:16][N:15]2[C:19](=[O:20])[C:12]=1/[N:11]=[C:27]1/[C:26]([NH:25][CH2:24][CH2:23][OH:22])=[CH:31][C:30](=[NH:35])[C:29]([O:33][CH3:34])=[CH:28]/1

Participants

7

Reactant 4

HCID 222AmmoniaHCID 784Hydrogen PeroxideHCID 158419865-[(2-Hydroxyethyl)amino]-2-methoxyphenolHCID 715878212,3-Diaminodihydropyrazolo pyrazolone dimethosulfonate

Product 1

HCID 178493061HCID 178493061, compound

Reagents, catalysts & solvents 2

HCID 702EthanolSolventHCID 962WaterSolvent

Procedure

0.05 mmol of 2,3-diamino-6,7-dihydro-1H,5H-pyrazolo[1,2-a]pyrazol-1-one dimethane sulfonate was dissolved in a mixture of water and ethanol (7.5 ml/1.5 ml). This solution was admixed with 0.05 mmol of 5-[(2-hydroxyethyl)amino]-2-methoxyphenol, then with 1.8 ml of concentrated aqueous ammonia, then with 9 ml of hydrogen peroxide.

Sources & evidence

ORD record
ord-519a437f37e94a20b5e4ed0bd4eeac77
Source dataset
uspto-grants-2009_09
Patent number
US07582123B2

Reaction notes

Loading…