HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 178428282, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | Hydrogen Peroxide | HCID 784 | — |
| Reactant | 5-Amino-6-Chloro-o-Cresol | HCID 157641 | — |
| Reactant | 8,9-diamino-3-methyl-2,3,4,5-tetrahydro-1H,7H-pyrazolo[1,2-a][1,2,5]triazepin-7-one methanesulfonate | HCID 86627738 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 178428282 | HCID 178428282 | — |
Reaction Steps
0.32 mmol of 8,9-diamino-3-methyl-2,3,4,5-tetrahydro-1H,7H-pyrazolo[1,2-a][1,2,5]triazepin-7-one methanesulfonate was dissolved in a mixture of water and ethanol (7.5 ml/1.5 ml). This solution was admixed with 0.32 mmol of 3-amino-2-chloro-6-methylphenol, then with 1.8 ml of concentrated aqueous ammonia, then with 9 ml of hydrogen peroxide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07582123B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-b6b0efa045aa4f269cba03dbff46ba5c |
| Source note | uspto-grants-2009_09 |