HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-(Morpholino)pyridin-3-amine → HCID 11495021, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-(Morpholino)pyridin-3-amine | HCID 104059 | — |
| Reactant | 4-Chloro-2-methyl-5-phenylisothiazol-3(2H)-one 1,1-dioxide | HCID 68662017 | — |
| Product | HCID 11495021 | HCID 11495021 | — |
Reaction Steps
The title compound was prepared from 4-chloro-2-methyl-5-phenylisothiazol-3(2H)-one 1,1-dioxide and 6-morpholin-4-ylpyridin-3-amine in a similar manner as described for Examples 9 and 13. 1H NMR (400 MHz, CD3CN): δ 3.20 (s, 3H), 3.26-3.30 (m, 4H), 3.65-3.70 (m, 4H), 6.31 (d, 1H), 6.94-6.99 (m, 1H), 7.11-7.22 (m, 4H), 7.25-7.30 (m, 1H), 7.58 (bs, 1H), 7.71 (d, 1H); Mass Spectrum: M−H+ 399.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07582629B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-35fe45b8e6be4f689639c8dcac8b709c |
| Source note | uspto-grants-2009_09 |