HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzenamine, 4-(4-morpholinyl)- → HCID 11590352, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzenamine, 4-(4-morpholinyl)- | HCID 75655 | — |
| Reactant | 4-Chloro-2-(2-methoxyethyl)-5-phenylisothiazol-3(2H)-one 1,1-dioxide | HCID 67243909 | — |
| Product | HCID 11590352 | HCID 11590352 | — |
Reaction Steps
The title compound was prepared from 4-chloro-2-(2-methoxyethyl)-5-phenylisothiazol-3(2H)-one 1,1-dioxide and 4-morpholin-4-ylaniline in a similar manner as described for Examples 9 and 13. 1H NMR (400 MHz, CD3CN): δ 2.92-2.97 (m, 4H), 3.38 (s, 3H), 3.70-3.75 (m, 6H), 3.90 (t, 2H), 6.51-6.56 (m, 2H), 6.68-6.72 (m, 2H), 7.08-7.16 (m, 4H), 7.22-7.27 (m, 1H), 7.67 (bs, 1H); Mass Spectrum: M+H+ 444.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07582629B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-dae9fa8e60444869bfe3741b60aef5e3 |
| Source note | uspto-grants-2009_09 |