HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonic Acid → HCID 86760942, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonic Acid | HCID 6395 | — |
| Reactant | 1-(5-tert-butyl-2-p-tolyl-2H-pyrazol-3-yl)-3-{1-[4-(2,2-dimethyl-propionyl)-piperazin-1-yl]-isoquinolin-4-yl}-urea | HCID 69052629 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 86760942 | HCID 86760942 | — |
Reaction Steps
Stir 1-(5-tert-butyl-2-p-tolyl-2H-pyrazol-3-yl)-3-{1-[4-(2,2-dimethyl-propionyl)-piperazin-1-yl]-isoquinolin-4-yl}-urea at room temperature. Add 1N methanesulfonic acid solution in dichloromethane to form the title compound. LCMS ES+ (m/z) 568 [M+H].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07582638B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-96d17d6f9df3449bab1d0a4b1aee0362 |
| Source note | uspto-grants-2009_09 |