HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyrrolidine → Pyrrolidine-1-sulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyrrolidine | HCID 31268 | — |
| Reactant | Sulfamide | HCID 82267 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | Pyrrolidine-1-sulfonamide | HCID 15707376 | — |
Reaction Steps
Pyrrolidine (3.37 g) and sulfamide (7.10 g) in 1,4-dioxane (110 ml) were heated at reflux for 24 h. The solvent was evaporated under reduced pressure and the resulting solid suspended in CHCl3. The suspension was filtered and the filtrate concentrated in vacuo to afford the subtitle compound as a white solid. Yield: 5.35 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07582644B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-7ead16268e084453b8f6d56e5118e8fb |
| Source note | uspto-grants-2009_09 |