HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylamine hydrochloride → HCID 21094217, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylamine hydrochloride | HCID 11198 | — |
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | HCID 21094067 | HCID 21094067 | — |
| Product | HCID 21094217 | HCID 21094217 | — |
Reaction Steps
4-[2-(Tetrahydropyran-4-yl)-1-(thiazol-2-ylcarbamoyl)ethyl]benzoic acid (Preparation 62, 150 mg, 420 μmol) was condensed with EtNH2.HCl in the presence of DIPEA, utilising the general procedure described in EXAMPLE 65, to give the title compound: RTA=2.97 min; m/z (ES+)=388.3 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07582632B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-ea73163662ee44f2b3feb35db9cfaaff |
| Source note | uspto-grants-2009_09 |