HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 178446133, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 178446132 | HCID 178446132 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 178446133 | HCID 178446133 | — |
Reaction Steps
Dissolve 126 mg (0.3 mmol) 5-[2-tert-butyl-5-(4-fluoro-phenyl)-1H-imidazol-4-yl]-3-(2,2-dimethyl-propyl)-3H-imidazo[4,5-b]pyridin-2-ylamine in 2.0 mL acetone. Add 120 μL of 5N hydrochloric acid incrementally. Filter the resultant precipitate. Air dry to provide 140 mg (93%) of very light pink crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07582652B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-5e384e7750e94191b662c0925113c0cd |
| Source note | uspto-grants-2009_09 |