HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aniline → HCID 178503386, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | HCID 178503385 | HCID 178503385 | — |
| Product | HCID 178503386 | HCID 178503386 | — |
Reaction Steps
Using the general method C, the title compound was prepared from 25b (0.2 g; 0.7 mmol) and aniline (0.65 g; 7.0 mmol) after a reaction time of 6 hours under reflux and separation by column chromatography (SiO2 60, CH2Cl2/EtOH 9+1). M.p. 228° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07582660B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-5d1c9f2c839c4f6d8bcacb0790b12a7e |
| Source note | uspto-grants-2009_09 |