Potassium Carbonate → HCID 15986635, compound

Participants

Reaction Steps

Compound 5k (0.42g, 0.98 mmol) was added to MeOH (10 mL), and K2CO3 (1 g) was added. The mixture was stirred for 3 h at rt. After that time, the solid was collected by vacuum filtration. The resulting filtrate was concentrated in vacuo. Water was added to the resulting residue and the mixture was stirred for 30 min. The solid was collected by vacuum filtration and purified by reverse phase HPLC to yield the title compound 44 (159 mg, 37%).

Provenance & Evidence