HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 9882765, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 21079266 | HCID 21079266 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 9882765 | HCID 9882765 | 109.3% |
Reaction Steps
0.7 ml of 2N HCl is added to a solution of 21 mg of butyl[6-chloro-5-phenyl-1-(2-(trimethylsilanyl)ethoxymethyl)-1H-indazol-3-yl]amine in 0.3 cm3 of methanol. The reaction medium is stirred at ambient temperature for 48 hours and at reflux for 1 hour, then evaporated. The solid obtained is dried under vacuum to give 16 mg of N-butyl-6-chloro-5-phenyl-1H-indazol-3-amine (yellow solid).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07582669B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-fc4699b446724dc6999c140145307749 |
| Source note | uspto-grants-2009_09 |