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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 730183Generated: October 29, 2026

Hydrochloric Acid → HCID 9882765, compound

https://huagongshe.com/reaction/730183

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 21079266HCID 21079266—
SolventMethanolHCID 887—
ProductHCID 9882765HCID 9882765109.3%

Reaction Steps

0.7 ml of 2N HCl is added to a solution of 21 mg of butyl[6-chloro-5-phenyl-1-(2-(trimethylsilanyl)ethoxymethyl)-1H-indazol-3-yl]amine in 0.3 cm3 of methanol. The reaction medium is stirred at ambient temperature for 48 hours and at reflux for 1 hour, then evaporated. The solid obtained is dried under vacuum to give 16 mg of N-butyl-6-chloro-5-phenyl-1H-indazol-3-amine (yellow solid).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07582669B2
Source datasetuspto-grants-2009_09
ORD IDord-fc4699b446724dc6999c140145307749
Source noteuspto-grants-2009_09