HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl acetimidate → HCID 178465587, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl acetimidate | HCID 26888 | — |
| Reactant | 3-amino-6-chloro-5-phenyl-1H-indazole | HCID 22319601 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 178465587 | HCID 178465587 | — |
Reaction Steps
33 mg of methyl acetimidate are added to 50 mg of 3-amino-6-chloro-5-phenyl-1H-indazole in 3 ml of acetonitrile and 12 mg of acetic acid. The reaction is placed under microwave radiation at 180° C. for 5 min. After the usual treatments and purification through silica, 35 mg of N-(6-chloro-5-phenyl-1H-indazol-3-yl)acetamidine are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07582669B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-3ea82e34c2b845758dad8ccb830fa13f |
| Source note | uspto-grants-2009_09 |