HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 57834521, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Benzo[b]thiophene-2-sulfonic acid (2-aminophenyl)amide | HCID 86240018 | — |
| Reactant | HCID 86605048 | HCID 86605048 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 57834521 | HCID 57834521 | 312.3% |
Reaction Steps
2-[2-(Benzo[b]thiophene-2-sulfonylamino) -phenylsulfamoyl]-6,7-dihydro-4H-thieno[3,2-c]pyridine-5-carboxylic acid tert-butyl ester (280 mg) was prepared by using 2-chlorosulfonyl-6,7-dihydro-4H-thieno[3,2-c]pyridine-5-carboxylic acid tert-butyl ester (0.049 g, 0.148 mmol) and benzo[b]thiophene-2-sulfonic acid (2-amino-phenyl)-amide (0.045 g, 0.148 mmol, prepared as in Example 1) using pyridine in DCM following procedure as in Example 2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07582673B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-5d8637c1fbea4b888758beea0a279c93 |
| Source note | uspto-grants-2009_09 |