HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 11753040, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 11455687 | HCID 11455687 | — |
| Product | HCID 11753040 | HCID 11753040 | 91% |
Reaction Steps
Using the procedure analogous to Example 5, from 2-[(2-{1-Ethyl-1-[4-(2-ethyl-2-hydroxy-butoxy)-3-methyl-phenyl]-propyl}-benzo[b]thiophene-6-carbonyl)-amino]-2-methyl-propionic acid methyl ester, example 30 (0.10 g, 0.18 mmol) and NaOH (0.036 g, 0.90 mmol) to furnish the titled compound (0.088 g, 0.016 mmol, 91%). LC/MS (m/z): calcd. for C31H41NO5S (M+H)+: 540.3; found: 540.3.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07582775B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-9873c5a9e3404430b988a4c6cffc2040 |
| Source note | uspto-grants-2009_09 |