Ammonium Chloride → HCID 178421937, compound

Participants

Reaction Steps

The desired product was prepared using a procedure similar to step 6 of example 3. Thus, [4-(1,3-dimethyl-2-phenyl-1H-indol-4-yl)-phenoxy]-acetonitrile (0.311 g, 0.882 mmol) was reacted with NaN3 (0.287 g, 4.412 mmol) and NH4Cl (0.236 g, 4.412 mmol) in DMF (5 ml) to give the product (0.246 g, 0.622 mmol, 71%) as a white solid, dec. 208-210° C.

Provenance & Evidence