HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 68817478, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Methyl bromoacetate | HCID 60984 | — |
| Reactant | HCID 68813887 | HCID 68813887 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 68817478 | HCID 68817478 | — |
Reaction Steps
The desired product was prepared using a procedure similar to step 1 of example 4. Thus, 4-(1,3-dimethyl-2-phenyl-1H-indol-4-yl)-phenol (0.300 g, 0.957 mmol) was reacted with K2CO3 (0.172 g, 1.244 mmol) and methyl bromoacetate (0.190 g, 1.244 mmol) in acetone (5 ml) to give the product (0.287 g, 0.745 mmol, 78%) as a white solid, mp 110-112° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07582773B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-5f0d4149138b4aa6aa7fd66e5af0d663 |
| Source note | uspto-grants-2009_09 |