反应详情

A mixture of 47.2 (11.1 mmol) and thionyl chloride (44 mmol) in DCM (20 mL) was stirred at room temperature overnight. After evaporation of solvent, 47.3 was obtained and it was used without further purification.

1. customAfter evaporation of solvent
2. custom47.3 was obtained
3. customit was used without further purification