HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 5-Bromo-1-chloro-2,3-dihydro-1H-indene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 5-bromo-2,3-dihydro-1H-inden-1-ol | HCID 13486299 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 5-Bromo-1-chloro-2,3-dihydro-1H-indene | HCID 22349515 | — |
Reaction Steps
A mixture of 47.2 (11.1 mmol) and thionyl chloride (44 mmol) in DCM (20 mL) was stirred at room temperature overnight. After evaporation of solvent, 47.3 was obtained and it was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07582803B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-5026e2f771874f2087328fd253aa1a6f |
| Source note | uspto-grants-2009_09 |