HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 178511557, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 178453951 | HCID 178453951 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 178511557 | HCID 178511557 | — |
Reaction Steps
380 mg of (trans-4-phenoxymethyl-cyclohexyl)-carbamic acid tert-butyl ester is dissolved in 5 mL of dichloromethane and 5 ml of trifluoroacetic acid is added. The mixture is stirred for 2 h, concentrated in vacuo and stripped twice from dichloromethane to afford 250 mg of trans-4-phenoxymethylcyclohexylamine trifluoroacetate as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07582769B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-e20eea23693847f4a2342f14a130a385 |
| Source note | uspto-grants-2009_09 |