HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 59186669, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 59186703 | HCID 59186703 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 59186669 | HCID 59186669 | 100% |
Reaction Steps
A solution of EXAMPLE 15D (0.51 g, 1.26 mmol) in dichloromethane (5 mL) at room temperature was treated with 2M HCl in diethyl ether (5 mL), stirred overnight, and concentrated to provide the desired product (0.38 g, 100%). MS (ESI) m/e 303 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07585858B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-c3cb7b80b60949d4ba2d12c0b487f348 |
| Source note | uspto-grants-2009_09 |