HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 2-aminopyridine-4-carboxylate → HCID 24738344, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 2-aminopyridine-4-carboxylate | HCID 236984 | — |
| Reactant | 4-(Bromoacetyl)-5-methyl-3-phenylisoxazole | HCID 2735531 | — |
| Product | HCID 24738344 | HCID 24738344 | 58% |
Reaction Steps
As described for Example 1, 4-(bromoacetyl)-5-methyl-3-phenylisoxazole (commercially available) (280 mg, 1.0 mmol) was converted, using methyl 2-aminopyridine-4-carboxylate instead of 2-aminopyridine, to the title compound (194 mg, 58%) which was obtained as a yellow foam. MS: m/e=334.1 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07585874B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-2fd31f736cd34c17b4092ca035167a9d |
| Source note | uspto-grants-2009_09 |