HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-5-chloropyridine → HCID 24738991, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-5-chloropyridine | HCID 66174 | — |
| Reactant | 4-(Bromoacetyl)-5-methyl-3-phenylisoxazole | HCID 2735531 | — |
| Product | HCID 24738991 | HCID 24738991 | 53% |
Reaction Steps
As described for Example 1, 4-(bromoacetyl)-5-methyl-3-phenylisoxazole (commercially available) (140 mg, 0.5 mmol) was converted, using 2-amino-5-chloropyridine instead of 2-aminopyridine, to the title compound (82 mg, 53%) which was obtained as a yellow gum. MS: m/e=310.3[M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07585874B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-b183fcedb85f44629f372d02523b21ec |
| Source note | uspto-grants-2009_09 |