HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-4-bromopyridine → HCID 24738828, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-4-bromopyridine | HCID 693282 | — |
| Reactant | 4-(Bromoacetyl)-5-methyl-3-phenylisoxazole | HCID 2735531 | — |
| Product | HCID 24738828 | HCID 24738828 | 33% |
Reaction Steps
As described for Example 2, 4-(bromoacetyl)-5-methyl-3-phenylisoxazole (commercially available) (2.0 g, 7.2 mmol) was converted, using 2-amino-4-bromopyridine instead of 2-amino-3-methylpyridine, to the title compound (824 mg, 33%) which was obtained as a light yellow foam. MS: m/e=354.1/355.9 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07585874B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-b6c0ffc1a63b4c718ae3196f7fc7fa65 |
| Source note | uspto-grants-2009_09 |