HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 57837445, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Thiourea | HCID 2723790 | — |
| Reactant | HCID 86637278 | HCID 86637278 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 57837445 | HCID 57837445 | 121% |
Reaction Steps
A mixture of 200 mg (0.63 mmol) of 2-chloro-1-(2-isopropylpyrazolo[1,5-a]pyridin-3-yl)ethanone, 100 mg of thiourea and 100 μl of HOAc were stirred in 1.5 ml of dioxane at 60-700 C for 30 minutes. 197 mg of 4-(2-isopropylpyrazolo[1,5-a]pyridin-3-yl)-1H-imidazole-2(3H)-thione was obtained after workup. Compound 1085.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07585875B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-27f0fe1911254de59af8affa7f92dc82 |
| Source note | uspto-grants-2009_09 |