HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thioglycolic Acid → HCID 22413933, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thioglycolic Acid | HCID 1133 | — |
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | m-Aminoacetanilide | HCID 7604 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-Nitrobenzenesulfonyl chloride | HCID 15540 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 22413933 | HCID 22413933 | — |
Reaction Steps
N-(3-Aminophenyl)acetamide was treated with 2-nitrophenylsulfonyl chloride in the presence of triethylamine and then the resulting compound was treated with iodomethane and potassium carbonate. Thereafter, the product was treated with thioglycolic acid to obtain N-[3-(methylamino)phenyl]acetamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07585878B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-32a054b2c9294b6797ba465de0d4ec3e |
| Source note | uspto-grants-2009_09 |