HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 57838010, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | 3-(Chloromethyl)-5-(3-chlorophenyl)-1,2,4-oxadiazole | HCID 10082520 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 57838010 | HCID 57838010 | 100% |
Reaction Steps
MeNH2 in EtOH (6 mL, 8 M, 48 mmol) was added to 3-(chloromethyl)-5-(3-chlorophenyl)-1,2,4-oxadiazole (1.5 g, 6.5 mmol) in EtOH (20 mL). After 20 h the solvent was evaporated and the residue was dried in vacuum to give 1.47 g (100%) of the title compound. LC-MS (M++1): 224
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07585881B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-4f65c854b1d24dd886049e2784158b3b |
| Source note | uspto-grants-2009_09 |