HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclopropyl isothiocyanate → HCID 57837972, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclopropyl isothiocyanate | HCID 92463 | — |
| Reactant | HCID 57838010 | HCID 57838010 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 57837972 | HCID 57837972 | 78% |
Reaction Steps
Cyclopropyl isothiocyanate (650 mg, 6.6 mmol) was added to 1-[5-(3-chlorophenyl)-[1,2,4]oxadiazol-3-yl]-N-methylmethanamine (1.47 g, 6.5 mmol) in EtOH (20 mL). After 3 h the formed precipitate was filtrated off and washed with cold EtOH to give 1.63 g (78%) of the title compound. LC-MS (M++1): 323.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07585881B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-6db1747ed73c4ba18da90187e29c4f9d |
| Source note | uspto-grants-2009_09 |