HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86600459, compound → 3-Phenylprop-2-enoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86600459 | HCID 86600459 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | 3-Phenylprop-2-enoyl chloride | HCID 66023 | — |
Reaction Steps
As further shown in FIG. 3, the cinnamoyl chloride aziridine intermediate was dissolved in aqueous acetic acid at 0° C., stirred at this temperature for 10 h and worked up as usual. Purification of the crude mixture by column chromatography and crystallization afforded the open chain cinnamoyl chloride intermediate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07585986B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-b617d0d5d762468ea81aa41c201e3b0c |
| Source note | uspto-grants-2009_09 |