HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → 1-Benzyl-5-oxopyrrolidine-3-carboaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 1-Benzyl-4-(hydroxymethyl)pyrrolidin-2-one | HCID 178824 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | 1-Benzyl-5-oxopyrrolidine-3-carboaldehyde | HCID 72299618 | — |
Reaction Steps
Triethylamine and a pyridine-sulfur trioxide complex were added to a DMSO solution of 1-benzyl-4-(hydroxymethyl)pyrrolidin-2-one and stirred at room temperature for 2Hours. Thereafter, its work-up and purification were carried out in the standard method to obtain 1-benzyl-5-oxopyrrolidine-3-carboaldehyde. EI: 203.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07585886B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-06587b7bb10048a493338260c3185964 |
| Source note | uspto-grants-2009_09 |