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HRID732669

反应详情

EQUATION

反应方程式

HRID 732669 的结构方程式

REACTANTS

反应物

2
结构：CCN(CC)CC
HCID8471

Triethylamine

C6H15N

结构：O=C1CC(CO)CN1Cc1ccccc1
HCID178824

1-Benzyl-4-(hydroxymethyl)pyrrolidin-2-one

C12H15NO2

PRODUCTS

生成物

1
结构：O=CC1CC(=O)N(Cc2ccccc2)C1
HCID72299618

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CS(C)=O
溶剂HCID679

Dimethyl sulfoxide

C2H6OS

PROCEDURE

实验过程

Triethylamine and a pyridine-sulfur trioxide complex were added to a DMSO solution of 1-benzyl-4-(hydroxymethyl)pyrrolidin-2-one and stirred at room temperature for 2Hours. Thereafter, its work-up and purification were carried out in the standard method to obtain 1-benzyl-5-oxopyrrolidine-3-carboaldehyde. EI: 203.

WORKUP

后处理

  1. customThereafter, its work-up and purification