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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 732743Generated: October 30, 2026

Hydrochloric Acid → HCID 68519472, compound

https://huagongshe.com/reaction/732743

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantDiethyl EtherHCID 3283—
ReactantHCID 59751427HCID 59751427—
SolventDichloromethaneHCID 6344—
ProductHCID 68519472HCID 6851947273%

Reaction Steps

Dissolve the compound of Example 9 (104 mg, 0.17 mmol) in dichloromethane (3 mL) and add 2M HCl in ether (400 μL, 0.8 mmol). Remove the solvent in vacuo to yield 81 mg of the title compound (73%): mass spectrum (ion spray): m/z=618.3 (M+H−HCl).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07585977B2
Source datasetuspto-grants-2009_09
ORD IDord-87e18fcbeae14fb7826d31649a26233c
Source noteuspto-grants-2009_09