Hydrochloric Acid → HCID 68518338, compound

HRID 732781Notes

Reaction equation

HRID 732781 reaction equation
[CH2:1]([S:3]([C:6]1[CH:7]=[C:8]([C:17]2[C:18]([O:28][C:29]3[CH:34]=[CH:33][C:32]([O:35][CH2:36][CH2:37][N:38]4[CH2:43][CH2:42][CH2:41][CH2:40][CH2:39]4)=[CH:31][CH:30]=3)=[C:19]3[C:24](=[CH:25][CH:26]=2)[CH:23]=[C:22]([OH:27])[CH:21]=[CH:20]3)[CH:9]=[C:10]([S:12]([CH2:15][CH3:16])(=[O:14])=[O:13])[CH:11]=1)(=[O:5])=[O:4])[CH3:2].[ClH:44]>ClCCl.CCOCC>[ClH:44].[CH2:1]([S:3]([C:6]1[CH:7]=[C:8]([C:17]2[C:18]([O:28][C:29]3[CH:34]=[CH:33][C:32]([O:35][CH2:36][CH2:37][N:38]4[CH2:39][CH2:40][CH2:41][CH2:42][CH2:43]4)=[CH:31][CH:30]=3)=[C:19]3[C:24](=[CH:25][CH:26]=2)[CH:23]=[C:22]([OH:27])[CH:21]=[CH:20]3)[CH:9]=[C:10]([S:12]([CH2:15][CH3:16])(=[O:14])=[O:13])[CH:11]=1)(=[O:5])=[O:4])[CH3:2]

Participants

5

Reactant 2

HCID 313Hydrochloric AcidHCID 68518339HCID 68518339, compound

Product 1

HCID 68518338HCID 68518338, compound

Reagents, catalysts & solvents 2

HCID 3283Diethyl EtherSolventHCID 6344DichloromethaneSolvent

Procedure

Dissolve the compound of Example 55 in dichloromethane and add 1N HCl in Et2O (0.180 mL). Evaporate to dryness to give the title compound.

Workup

  1. customEvaporate to dryness

Sources & evidence

ORD record
ord-303f1f0bc59b4d80b867addf17978f17
Source dataset
uspto-grants-2009_09
Patent number
US07585977B2

Reaction notes

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