HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbonochloridic acid, 4-methoxyphenyl ester → HCID 57838934, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbonochloridic acid, 4-methoxyphenyl ester | HCID 82128 | — |
| Reactant | Tert-butyl 4-(prop-2-yn-1-yl)piperidine-1-carboxylate | HCID 18187546 | — |
| Product | HCID 57838934 | HCID 57838934 | — |
Reaction Steps
4-(methoxy)phenyl chloroformate (5.00 g, 26.8 mmol) was added to a solution of tert-butyl 4-(prop-2-ynyl)piperidine-1-carboxylate (4.60 g, 20.9 mmol) according to general procedure 1. Yield=5.02 g, 90%. m/z MH+=274.06. HPLC rt=12.2 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07589076B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-6bad77878d444749bea8763b9cb0b60a |
| Source note | uspto-grants-2009_09 |