HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Nitrobenzyl chloroformate → HCID 57838932, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Nitrobenzyl chloroformate | HCID 78205 | — |
| Reactant | Tert-butyl 4-(prop-2-yn-1-yl)piperidine-1-carboxylate | HCID 18187546 | — |
| Product | HCID 57838932 | HCID 57838932 | — |
Reaction Steps
4-(nitro)benzyl chloroformate (5.00 g, 23.2 mmol) was added to a solution of tert-butyl 4-(prop-2-ynyl)piperidine-1-carboxylate (3.98 g, 17.4 mmol) according to general procedure 1. Yield=4.66 g, 86%. m/z MH+=302.98. HPLC rt=12.3 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07589076B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-d2858376e0854d71abc4c8f5a90e4c73 |
| Source note | uspto-grants-2009_09 |