HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 178508313, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 178504231 | HCID 178504231 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178508313 | HCID 178508313 | 104.1% |
Reaction Steps
A solution of 7-(1-(2-(trimethylsilyl)ethoxymethyl)-1H-pyrazol-3-yl)-1H-[1,2,3]triazolo[4,5-d]pyrimidine-5-amine (120 mg, 0.361 mmol) in MeOH (2 mL) was treated with HCl (4-M in dioxan, 1 mL), stirred for 2 h, filtered and the resulting solid washed with Et2O to give the title compound (76 mg, 100%) as a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07589097B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-de282914200d40ba956dd0054fc4274b |
| Source note | uspto-grants-2009_09 |