HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 10288897, compound → HCID 10237550, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 10288897 | HCID 10288897 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 10237550 | HCID 10237550 | — |
Reaction Steps
A solution of hydroxamic acid 7 (100 mg, 0.21 mmol) in 20 ml of methanol was hydrogenated under normal pressure with 50 mg of palladium on barium sulfate for about 5 hours. After filtration of the catalyst the solvent was evaporated and the crude product was purified by preparative HPLC to give a white solid. Yield: 53 mg (65%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07589091B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-e6fb92a8e4344daeb4c4c309312235bd |
| Source note | uspto-grants-2009_09 |