HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzenepropanoyl chloride → ethyl (2E)-3-{4-[(4-dec-1-ynylbenzyl)(3-phenylpropanoyl)-amino]phenyl}acrylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzenepropanoyl chloride | HCID 64801 | — |
| Reactant | ethyl (2E)-3-{4-[(4-dec-1-ynylbenzyl)amino)phenyl}acrylate | HCID 11200896 | — |
| Product | ethyl (2E)-3-{4-[(4-dec-1-ynylbenzyl)(3-phenylpropanoyl)-amino]phenyl}acrylate | HCID 86612441 | — |
Reaction Steps
The title compound was prepared following the procedure E using of ethyl (2E)-3-{4-[(4-dec-1-ynylbenzyl)amino]phenyl}acrylate and 3-phenylpropanoyl chloride (58%). M+ (ESI): 560.6. HPLC, Rt: 6.4 min (purity: 98.7%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07589232B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-157d556a67a3415cb4c22b39522c5f6b |
| Source note | uspto-grants-2009_09 |