HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → ethyl (2E)-3-{4-[acetyl(4-dec-1-ynylbenzyl)amino]phenyl}acrylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | ethyl (2E)-3-{4-[(4-dec-1-ynylbenzyl)amino)phenyl}acrylate | HCID 11200896 | — |
| Product | ethyl (2E)-3-{4-[acetyl(4-dec-1-ynylbenzyl)amino]phenyl}acrylate | HCID 57841323 | — |
Reaction Steps
The title compound was prepared following the procedure E using ethyl (2E)-3-{4-[(4-dec-1-ynylbenzyl)amino]phenyl}acrylate and acetyl chloride as a yellow oil (97%). M+ (ESI): 460.2. HPLC, Rt: 6.0 min (purity: 98.8%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07589232B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-38fc05c73458452790ffcbbd6b4b4411 |
| Source note | uspto-grants-2009_09 |