HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyloxyacetyl chloride → HCID 57841363, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyloxyacetyl chloride | HCID 177085 | — |
| Reactant | 6-({4-[(4-butylphenyl)ethynyl]benzyl}amino)-2,2-dimethyl-4H-1,3-benzodioxin-4-one hydrochloride | HCID 68419698 | — |
| Product | HCID 57841363 | HCID 57841363 | — |
Reaction Steps
The titled compound was prepared following the procedure K using 6-({4-[(4-butylphenyl)ethynyl]benzyl}amino)-2,2-dimethyl-4H-1,3-benzodioxin-4-one hydrochloride and (benzyloxy)acetyl chloride as a yellow oil (88%). M+ (ESI): 588.5. HPLC, Rt: 5.76 min (Purity: 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07589232B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-4ea38703be404b14a47118f87258d778 |
| Source note | uspto-grants-2009_09 |