HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzo[b]thiophene-2-carbonyl Chloride → HCID 57841380, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzo[b]thiophene-2-carbonyl Chloride | HCID 142384 | — |
| Reactant | 6-({4-[(4-butylphenyl)ethynyl]benzyl}amino)-2,2-dimethyl-4H-1,3-benzodioxin-4-one hydrochloride | HCID 68419698 | — |
| Product | HCID 57841380 | HCID 57841380 | — |
Reaction Steps
The titled compound was prepared following the procedure K using 6-({4-[(4-butylphenyl)ethynyl]benzyl}amino)-2,2-dimethyl-4H-1,3-benzodioxin-4-one hydrochloride and 1-benzothiophene-2-carbonyl chloride as a yellow oil (95%). HPLC, Rt: 6.04 min (Purity: 92.1%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07589232B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-21cfae537ca0420f8c6bdca3c85f57d1 |
| Source note | uspto-grants-2009_09 |