HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyanoacetic acid → HCID 57841361, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyanoacetic acid | HCID 9740 | — |
| Reactant | Methyl {4-[({4-[(4-butylphenyl)ethynyl]benzyl}amino)methyl]phenoxy}acetate | HCID 57554567 | — |
| Product | HCID 57841361 | HCID 57841361 | — |
Reaction Steps
The titled compound was prepared following the procedure H using methyl {4-[({4-[(4-butylphenyl)ethynyl]benzyl}amino)methyl]phenoxy}acetate and cyanoacetic acid, as a pale yellow oil (96%). M− (ESI): 507.4; M+ (ESI): 509.4. HPLC, Rt: 5.22 min (Purity: 86.2%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07589232B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-d6a6e985af924e6aab5630848b472da7 |
| Source note | uspto-grants-2009_09 |