HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 11167834, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 57841361 | HCID 57841361 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 11167834 | HCID 11167834 | — |
Reaction Steps
The titled compound was prepared following the procedure F using methyl (4-{[{4-[(4-butylphenyl)ethynyl]benzyl}(cyanoacetyl)amino]methyl}phenoxy)acetate and NaOH 1 N in the presence of DMF, as a white powder (20%). M− (ESI): 493.3; M+ (ESI): 495.3. HPLC, Rt: 5.01 min (Purity: 80.6%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07589232B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-dff3919179c84895a4f0e6f60948ae44 |
| Source note | uspto-grants-2009_09 |