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HRID733575

反应详情

EQUATION

反应方程式

HRID 733575 的结构方程式

REACTANTS

反应物

2
反应SMILES：[Na+].[OH-]
HCID14798

Sodium Hydroxide

HNaO

反应SMILES：CCCCc1ccc(C#Cc2ccc(CN(Cc3ccc(OCC(=O)OC)cc3)C(=O)CC#N)cc2)cc1
HCID57841361

未命名化合物

PRODUCTS

产物

1
反应SMILES：CCCCc1ccc(C#Cc2ccc(CN(Cc3ccc(OCC(=O)O)cc3)C(=O)CC#N)cc2)cc1
HCID11167834

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
反应SMILES：CN(C)C=O
溶剂HCID6228

Dimethylformamide

C3H7NO

PROCEDURE

实验过程

The titled compound was prepared following the procedure F using methyl (4-{[{4-[(4-butylphenyl)ethynyl]benzyl}(cyanoacetyl)amino]methyl}phenoxy)acetate and NaOH 1 N in the presence of DMF, as a white powder (20%). M− (ESI): 493.3; M+ (ESI): 495.3. HPLC, Rt: 5.01 min (Purity: 80.6%).